In Situ Synchrotron Radiation Techniques: Watching Deformation-induced Structural Evolutions of Polymers

Synchrotron radiation induced TXRF†

The use of synchrotron radiation (SR) as an excitation source for total reflection X-ray fluorescence analysis (TXRF) offers several advantages over X-ray tube excitation. Detection limits in the fg range can be achieved with efficient excitation for low Z as well as high Z elements due to the features of synchrotron radiation and in particular the high brilliance in a wide spectral range and t...

Deformation mechanisms of twinning-induced plasticity steels: In situ synchrotron characterization and modeling

The plastic deformation behavior of twinning-induced plasticity steels of composition Fe–25Mn–3Si–3Al are investigated by means of in situ synchrotron high-energy X-ray diffraction and compared to self-consistent simulations. It is the first time the alternating interaction of {1 1 1} <1 1 0> slip and {1 1 1} <1 1 2> twinning have been directly observed in situ while undergoing uniaxial tension...

In situ visualization of thermal distortions of synchrotron radiation optics

We have developed a new in situ method to measure heating-induced distortions of the surface of the first monochromator crystal exposed to high-power white synchrotron radiation beam. The method is based on recording the image of a stationary grid of dots captured by a CCD camera as reflected from the surface of a crystal with and without a heat load. The three-dimensional surface profile (heat...

Glycoscience@Synchrotron: Synchrotron radiation applied to structural glycoscience

Synchrotron radiation is the most versatile way to explore biological materials in different states: monocrystalline, polycrystalline, solution, colloids and multiscale architectures. Steady improvements in instrumentation have made synchrotrons the most flexible intense X-ray source. The wide range of applications of synchrotron radiation is commensurate with the structural diversity and compl...

Electric field-induced deformation of polydimethylsiloxane polymers